4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one

Base Information

• Chemical Name: 4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one
• CAS No.: 2363-99-7
• Molecular Formula: C20H20 N2 O
• Molecular Weight: 304.392
• Hs Code.: 2925290090
• European Community (EC) Number: 219-118-0
• DSSTox Substance ID: DTXSID901211970
• Nikkaji Number: J84.893J
• Mol file: 2363-99-7.mol

Synonyms:2363-99-7;4-[4-(diethylamino)phenyl]iminonaphthalen-1-one;4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one;EINECS 219-118-0;1(4H)-Naphthalenone, 4-[[4-(diethylamino)phenyl]imino]-;4-[[4-(DIETHYLAMINO)PHENYL]IMINO]NAPHTHALEN-1(4H)-ONE;SCHEMBL1896739;SCHEMBL5509539;DTXSID901211970;AKOS024385307;C.I.49705;1,4-Naphthoquinone imine, N-[p-(diethylamino)phenyl]-;4-[[4-(Diethylamino)phenyl]imino]-1(4H)-naphthalenone

Chemical Property of 4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one

Chemical Property:

• Vapor Pressure: 2.45E-08mmHg at 25°C
• Melting Point: 114-117 °C
• Boiling Point: 451.4°Cat760mmHg
• PKA: 4.75±0.32(Predicted)
• Flash Point: 226.8°C
• PSA: 32.67000
• Density: 1.08g/cm³
• LogP: 4.40610
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 304.157563266
• Heavy Atom Count: 23
• Complexity: 470

Purity/Quality:

99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)C1=CC=C(C=C1)N=C2C=CC(=O)C3=CC=CC=C23

Technology Process of 4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one

There total 3 articles about 4-((4-(Diethylamino)phenyl)imino)naphthalen-1(4H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

α-naphthol (90-15-3) + N,N-diethylaniline (93-05-0) → 4-[[4-(diethylamino)phenyl]imino]-1(4H)-naphthalenone (2363-99-7)

Guidance literature:

In acetonitrile; at 25 ℃; pH=8; aq. phosphate buffer; Electrochemical reaction;

DOI:10.1021/ol103146k

Reference yield:

→ 4-[[4-(diethylamino)phenyl]imino]-1(4H)-naphthalenone (2363-99-7)

Guidance literature:

Naphthol-(1), p-Amino-N,N-diaethyl-anilin, H2O2, Fe-III-Aethylendiamin-tetraessigsaeure(EDTA)-Komplex (Mechanismus);

DOI:10.1021/ja01496a068

Reference yield:

→ 4-{[4-(diethylamino)phenyl]imino}naphthalen-1(4H)-one (2363-99-7)

Guidance literature:

upstream raw materials:

α-naphthol

N,N-diethylaniline

Refernces

• 1、 Maleki, Abbas,Nematollahi, Davood. "Electrochemical synthesis and mechanestic study of quinone imines exploiting the dual character of N,N-dialkyl-p-phenylenediamines". supporting information; experimental part. p. 1928 - 1931. Retrieved 2011/06/21.