[1,1'-Binaphthalene]-8,8'-dicarboxylic acid

Base Information

• Chemical Name: [1,1'-Binaphthalene]-8,8'-dicarboxylic acid
• CAS No.: 29878-91-9
• Deprecated CAS: 117-16-8,126721-57-1,50870-01-4,126721-57-1,50870-01-4
• Molecular Formula: C₂₂H₁₄O₄
• Molecular Weight: 342.351
• European Community (EC) Number: 249-922-7
• NSC Number: 7810
• UNII: 9TV2DT592L
• DSSTox Substance ID: DTXSID8067525
• Nikkaji Number: J40.549C
• Wikidata: Q72443486
• ChEMBL ID: CHEMBL1604468
• Mol file: 29878-91-9.mol

Synonyms:29878-91-9;[1,1'-Binaphthalene]-8,8'-dicarboxylic acid;Dina acid;1,1'-Binaphthyl-8,8'-dicarboxylic acid;[1,1']Binaphthalenyl-8,8'-dicarboxylic acid;8-(8-carboxynaphthalen-1-yl)naphthalene-1-carboxylic acid;NSC7810;NSC-7810;9TV2DT592L;(1,1'-Binaphthalene)-8,8'-dicarboxylic acid;NSC 7810;EINECS 249-922-7;1,1'-Binaphthalene-8,8'-dicarboxylic acid;EC 249-922-7;Compound P7810;1,8'-dicarboxylic acid;Maybridge1_002277;[1,1'-Binaphthalene]-8,8'-dicarboxylicacid;[1,8'-dicarboxylic acid;NCIStruc1_001210;NCIStruc2_000874;UNII-9TV2DT592L;SCHEMBL1449076;CHEMBL1604468;DTXSID8067525;BDBM26615;HMS547P11;NCI7810;8,8'-dicarboxy-1,1'-binaphthyl;CCG-36341;NCGC00013086;STL483067;4,5-Dichloro-1,8-naphthalicanhydride;AKOS000114527;NCGC00013086-02;NCGC00096209-01;NCI60_041722;CS-0218078;FT-0606057;EN300-00055;W-110768;Z56785528;F0020-1849;[1,1 inverted exclamation marka-Binaphthalene]-8,8 inverted exclamation marka-dicarboxylic acid

Chemical Property of [1,1'-Binaphthalene]-8,8'-dicarboxylic acid

Chemical Property:

• Melting Point: 306-307℃
• Boiling Point: 615.7±40.0 °C(Predicted)
• PKA: 2.68±0.10(Predicted)
• Flash Point: 340.2oC
• PSA: 74.60000
• Density: 1.380±0.06 g/cm3 (20 ºC 760 Torr)
• LogP: 5.05640
• XLogP3: 5.1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 342.08920892
• Heavy Atom Count: 26
• Complexity: 496

Purity/Quality:

99.9% ^*data from raw suppliers

1,1'-BINAPHTHYL-8,8'-DICARBOXYLIC ACID Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC2=C(C(=C1)C3=CC=CC4=C3C(=CC=C4)C(=O)O)C(=CC=C2)C(=O)O

Technology Process of [1,1'-Binaphthalene]-8,8'-dicarboxylic acid

There total 8 articles about [1,1'-Binaphthalene]-8,8'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.35%

1,8-naphtholactam (130-00-7) → [1,1']binaphthyl-8,8'-dicarboxylic acid (10507-64-9,10507-65-0,29878-91-9,50870-01-4)

Guidance literature:

1,8-naphtholactam; With sodium hydroxide; In water; at 100 ℃; for 4h; pH=10;

With hydrogenchloride; sodium nitrite; In water; at 3 ℃; for 2.5h;

With ammonium hydroxide; hydroxylamine hydrochloride; copper(l) chloride; Reagent/catalyst;

Reference yield:

→ [1,1']binaphthyl-8,8'-dicarboxylic acid (10507-64-9,10507-65-0,29878-91-9,50870-01-4)

Guidance literature:

With potassium hydroxide; pentan-1-ol;

DOI:10.1021/ja01359a038

Reference yield:

→ [1,1']binaphthyl-8,8'-dicarboxylic acid (10507-64-9,10507-65-0,29878-91-9,50870-01-4)

Guidance literature:

With copper(I) oxide;

upstream raw materials:

1,8-naphtholactam

Downstream raw materials:

anthanthrone

7-Oxo-dibenzanthracen

7-oxo-7H-dibenzo[a,kl]anthracene-13-carboxylic acid

Refernces