Technology Process of C24H25N3O3S
There total 9 articles about C24H25N3O3S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrahydrofuran; water
2: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
3: water; N-ethyl-N,N-diisopropylamine / 1,2-dimethoxyethane / 24 h / Reflux
With
water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.12.040
- Guidance literature:
-
With
water; N-ethyl-N,N-diisopropylamine;
In
1,2-dimethoxyethane;
for 24h;
Reflux;
DOI:10.1016/j.bmc.2011.12.040
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride / toluene / Heating
2: ammonia / methanol
3: pyridine; trifluoroacetic anhydride
4: lithium hydroxide / tetrahydrofuran; water
5: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide
6: water; N-ethyl-N,N-diisopropylamine / 1,2-dimethoxyethane / 24 h / Reflux
With
pyridine; thionyl chloride; ammonia; water; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; trifluoroacetic anhydride; lithium hydroxide;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmc.2011.12.040