Sodium 2,4,6-trinitrophenate

Base Information

• Chemical Name: Sodium 2,4,6-trinitrophenate
• CAS No.: 3324-58-1
• Molecular Formula: C6H3 N3 O7 . Na
• Molecular Weight: 251.088
• Hs Code.: 2908999090
• Mol file: 3324-58-1.mol

Synonyms:Phenol,2,4,6-trinitro-, sodium salt (9CI); Picric acid, sodium deriv. (6CI); Picricacid, sodium salt (8CI); Sodium, (picryloxy)- (7CI); Sodium2,4,6-trinitrophenolate; Sodium picrate; Sodium trinitrophenolate

Chemical Property of Sodium 2,4,6-trinitrophenate

Chemical Property:

• Vapor Pressure: 0.000514mmHg at 25°C
• Melting Point: 122-123oC
• Boiling Point: 303.6°Cat760mmHg
• Flash Point: 133.9°C
• PSA: 160.52000
• Density: 1.856g/cm³
• LogP: 3.12460

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Sodium 2,4,6-trinitrophenate

There total 43 articles about Sodium 2,4,6-trinitrophenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.8%

2,4,6-Trinitrophenol (88-89-1) → sodium picrate (3324-58-1)

Guidance literature:

With sodium hydroxide; In ethanol; at 20 ℃; for 2h;

Reference yield: 87.0%

2,4,6-trinitrochlorobenzene (88-88-0) → sodium picrate (3324-58-1)

Guidance literature:

With Cumene hydroperoxide; cumene hydroperoxide sodium salt; In toluene; for 24h; Ambient temperature;

Reference yield:

4-nitro-benzaldehyde-(O-picryl-seqtrans-oxime ) (115828-63-2) → sodium picrate (3324-58-1) + 4-nitrobenzonitrile (619-72-7)

Guidance literature:

With sodium methylate; In methanol; at 25 ℃; Rate constant;

DOI:10.1021/ja00035a040

upstream raw materials:

sodium methylate

1,2,3,5-tetranitrobenzene

1,3,5-trinitrobenzene

2,4,6-trinitrochlorobenzene

Downstream raw materials:

picramic acid

sodium trichloroacetate

Refernces

• 1、 Li, Ning,Chen, Feng,Shen, Jie,Zhang, Hao,Wang, Tianxiang,Ye, Ruijuan,Li, Tianhu,Loh, Teck Peng,Yang, Yi Yan,Zeng, Huaqiang. "Buckyball-Based Spherical Display of Crown Ethers for de Novo Custom Design of Ion Transport Selectivity". supporting information. p. 21082 - 21090. Retrieved 2020/12/21.
• 2、 Marcos, Paula M.,Ascenso, José R.,Segurado, Manuel A.P.,Bernardino, Raul J.,Cragg, Peter J.. "Synthesis, binding properties and theoretical studies of p-tert-butylhexahomotrioxacalix[3]arene tri(adamantyl)ketone with alkali, alkaline earth, transition, heavy metal and lanthanide cations". experimental part. p. 496 - 503. Retrieved 2009/04/07.