sec-butyl-3-phenylpropionate

Base Information

• Chemical Name: sec-butyl-3-phenylpropionate
• CAS No.: 51869-23-9
• Molecular Formula: C₁₃H₁₈O₂
• Molecular Weight: 206.285
• Mol file: 51869-23-9.mol

Synonyms:sec-butyl-3-phenylpropionate

Chemical Property of sec-butyl-3-phenylpropionate

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of sec-butyl-3-phenylpropionate

There total 15 articles about sec-butyl-3-phenylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

ethyl dihydrocinnamate (2021-28-5) + iso-butanol (78-92-2,15892-23-6) → ethanol (64-17-5) + sec-butyl-3-phenylpropionate (51869-23-9)

Guidance literature:

2[{Cl(C₆F₁₃CH₂CH₂)2SnOSn(CH₂CH₂C₆F₁₃)2Cl}2]; In various solvent(s); at 150 ℃; for 16h;

DOI:10.1002/1521-3773(20011001)40:19<3670::AID-ANIE3670>3.0.CO;2-9

Reference yield: 100.0%

ethyl dihydrocinnamate (2021-28-5) + iso-butanol (78-92-2,15892-23-6) → sec-butyl-3-phenylpropionate (51869-23-9)

Guidance literature:

[Cl(C₆F₁₃C₂H₄)2SnOSn(C₂H₄C₆F₁₃)2Cl]2; In various solvent(s); at 150 ℃; for 16h;

DOI:10.1002/1615-4169(200201)344:1<84::AID-ADSC84>3.0.CO;2-C

Reference yield: 90.0%

3-Phenyl-propionic acid 2-mercapto-1-methyl-propyl ester → sec-butyl-3-phenylpropionate (51869-23-9)

Guidance literature:

With tri-n-butyl-tin hydride; for 5h;

DOI:10.1021/ja00371a054

upstream raw materials:

4,4-dimethyl-2-(2-phenylethyl)-4,5-dihydro-1,3-oxazole

iso-butanol

3-phenyl-1-(2-thioxothiazolidin-3-yl)propan-1-one

ethyl dihydrocinnamate

Refernces

• 1、 Guissart, Céline,Barros, Andre,Rosa Barata, Luis,Evano, Gwilherm. "Broadly Applicable Ytterbium-Catalyzed Esterification, Hydrolysis, and Amidation of Imides". supporting information. p. 5098 - 5102. Retrieved 2018/09/13.
• 2、 Tschaen, Brittany A.,Schmink, Jason R.,Molander, Gary A.. "Pd-catalyzed aldehyde to ester conversion: A hydrogen transfer approach". supporting information. p. 500 - 503. Retrieved 2013/04/11.