potassium salt of phenyldinitromethane

Base Information

• Chemical Name: potassium salt of phenyldinitromethane
• CAS No.: 28198-51-8
• Molecular Formula: C₇H₅N₂O₄*K
• Molecular Weight: 220.226
• Mol file: 28198-51-8.mol

Synonyms:potassium salt of phenyldinitromethane

Chemical Property of potassium salt of phenyldinitromethane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of potassium salt of phenyldinitromethane

There total 2 articles about potassium salt of phenyldinitromethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

C7H5AgN2O2 → potassium salt of phenyldinitromethane (28198-51-8)

Guidance literature:

With dipotassium hydrogenphosphate; formic acid; dihydrogen peroxide; In water; at 0 - 45 ℃;

DOI:10.1016/j.mencom.2010.06.011

Reference yield:

→ potassium salt of phenyldinitromethane (28198-51-8)

Guidance literature:

Benzaldoxim, 1) N2O4, 2) KOH ;

Reference yield:

potassium salt of phenyldinitromethane (28198-51-8) + Diethyl maleate (141-05-9) → (4RS,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester (57065-93-7,57065-94-8,91154-16-4)

Guidance literature:

In N,N-dimethyl-formamide; at 80 ℃; for 24h;

DOI:10.1021/jo00863a027

Downstream raw materials:

(4RS,5RS)-3-phenyl-4,5-dihydro-isoxazole-4,5-dicarboxylic acid diethyl ester

3-phenyl-5-acetoxy-4,5-dihydroisoxazole

(+/-)-ethyl 3-phenyl-4,5-dihydroisoxazole-5-carboxylate

dimethyl 3-phenyl-4,5-dihydroisoxazole-4,5-dicarboxylate

Refernces