Technology Process of C18H28O3
There total 5 articles about C18H28O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diisobutylaluminium hydride;
In
tetrahydrofuran; dichloromethane;
at -78 ℃;
for 2h;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 21 h / 0 - 20 °C
2: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2 h / -78 °C
With
diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1021/ol3017676
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 °C
1.2: 18 h / 0 - 20 °C
2.1: pyridine; sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 5.5 h / 0 - 20 °C
3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / acetonitrile / 21 h / 0 - 20 °C
4.1: diisobutylaluminium hydride / tetrahydrofuran; dichloromethane / 2 h / -78 °C
With
pyridine; sulfur trioxide pyridine complex; sodium hydride; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; lithium chloride;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; acetonitrile; mineral oil;
2.1: Parikh-Doering oxidation;
DOI:10.1021/ol3017676