Diels-Alder adduct

Base Information

• Chemical Name: Diels-Alder adduct
• CAS No.: 5205-63-0
• Molecular Formula: C₁₄H₂₃NO₄
• Molecular Weight: 269.341
• Mol file: 5205-63-0.mol

Synonyms:Diels-Alder adduct

Chemical Property of Diels-Alder adduct

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of Diels-Alder adduct

There total 1 articles about Diels-Alder adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-ethoxy-4-methyl-oxazole (5006-20-2) + 2-isopropyl-4,7-dihydro-[1,3]dioxepine (5417-35-6) → Diels-Alder adduct (5205-63-0) + ethyl 2-isocyanopropionate (33140-27-1) + 4,5'-O-isobutylidenepyridoxine (1622-67-9)

Guidance literature:

at 90 - 155 ℃; for 4 - 24h; under 112.511 - 760.051 Torr; Product distribution / selectivity;

Reference yield: 98.0%

Diels-Alder adduct (5205-63-0) → 4,5'-O-isobutylidenepyridoxine (1622-67-9)

Guidance literature:

With acetic acid; at 80 - 92 ℃; for 2.75h; under 225.023 - 760.051 Torr;

Reference yield: 86.05%

Diels-Alder adduct (5205-63-0) → pyridoxal hydrochloride (58-56-0)

Guidance literature:

Diels-Alder adduct; With hydrogenchloride; In ethanol; water; at 20 ℃; for 2h;

In ethanol; water; for 2h;

upstream raw materials:

5-ethoxy-4-methyl-oxazole

2-isopropyl-4,7-dihydro-[1,3]dioxepine

Downstream raw materials:

4,5'-O-isobutylidenepyridoxine

pyridoxal hydrochloride

Refernces