FmocGlu(OtBu)NH(CH₂)4NHZ

Base Information

• Chemical Name: FmocGlu(OtBu)NH(CH₂)4NHZ
• CAS No.: 1228766-30-0
• Molecular Formula: C₃₆H₄₃N₃O₇
• Molecular Weight: 629.753
• Mol file: 1228766-30-0.mol

Synonyms:FmocGlu(OtBu)NH(CH₂)4NHZ

Chemical Property of FmocGlu(OtBu)NH(CH₂)4NHZ

Chemical Property:

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Technology Process of FmocGlu(OtBu)NH(CH₂)4NHZ

There total 1 articles about FmocGlu(OtBu)NH(CH₂)4NHZ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

(4-aminobutyl)carbamic acid benzyl ester (62146-62-7) + Nα-Fmoc-Glu-(O-tBu)-OPfp (86061-04-3,200616-21-3) → FmocGlu(OtBu)NH(CH2)4NHZ (1228766-30-0)

Guidance literature:

With benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In dichloromethane;

DOI:10.1007/s00726-009-0337-5

Reference yield:

FmocGlu(OtBu)NH(CH2)4NHZ (1228766-30-0) → C32H35N3O7 (1228766-35-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1007/s00726-009-0337-5

upstream raw materials:

(4-aminobutyl)carbamic acid benzyl ester

N^α-Fmoc-Glu-(O-tBu)-OPfp

Downstream raw materials:

C₃₂H₃₅N₃O₇

Refernces