1-CYCLOPROPYLETHANOL ACETATE

Base Information

• Chemical Name: 1-CYCLOPROPYLETHANOL ACETATE
• CAS No.: 7515-52-8
• Molecular Formula: C₇H₁₂O₂
• Molecular Weight: 128.171
• Mol file: 7515-52-8.mol

Synonyms:Cyclopropanemethanol,a-methyl-, acetate(6CI,7CI,8CI,9CI); NSC 54298

Chemical Property of 1-CYCLOPROPYLETHANOL ACETATE

Chemical Property:

• Vapor Pressure: 5.51mmHg at 25°C
• Boiling Point: 142.7°C at 760 mmHg
• Flash Point: 34.3°C
• PSA: 26.30000
• Density: 1.022g/cm³
• LogP: 1.34800

Purity/Quality:

99% ^*data from raw suppliers

1-CYCLOPROPYL ETHANOL ACETATE 98.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-CYCLOPROPYLETHANOL ACETATE

There total 7 articles about 1-CYCLOPROPYLETHANOL ACETATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

(Z)-1-iodo-3-pentene (66688-64-0) + silver(I) acetate (563-63-3) → 1-cyclopropyl-1-ethanol acetate (7515-52-8,141632-28-2) + 5-Acetoxy-(Z)-2-pentene (42125-19-9)

Guidance literature:

In benzene; at 25 ℃; for 8h;

DOI:10.1016/S0040-4039(01)80138-6

Reference yield:

1-cyclopropylethanol (765-42-4) + acetic anhydride (108-24-7) → 1-cyclopropyl-1-ethanol acetate (7515-52-8,141632-28-2)

Guidance literature:

at 190 ℃;

Reference yield:

Cyclopropyl methyl ketone (765-43-5) → 1-cyclopropyl-1-ethanol acetate (7515-52-8,141632-28-2)

Guidance literature:

Multi-step reaction with 2 steps

1: LiAlH₄

2: NaOAc

With lithium aluminium tetrahydride; sodium acetate;

DOI:10.1021/ja01503a036

upstream raw materials:

1-cyclopropylethanol

acetic anhydride

(Z)-1-iodo-3-pentene

silver(I) acetate

Downstream raw materials:

5-Methyl-5-nonanol

n-hexan-2-one

1-cyclopropylethanol

(E)-3-penten-1-ol

Refernces

• 1、 Previtera, Lucio,Monaco, Pietro,Mangoni, Lorenzo. "CYCLOPROPYLCARBINYL COMPOUNDS FROM HOMOALLYLIC IODIDES". . p. 1293 - 1294. Retrieved 2007/10/02.