(Z)-2-lithio-1-(o-lithiophenyl)ethene dimer

Base Information

• Chemical Name: (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer
• CAS No.: 143077-02-5
• Molecular Formula: C₈H₆Li₂
• Molecular Weight: 116.018
• Mol file: 143077-02-5.mol

Synonyms:(Z)-2-lithio-1-(o-lithiophenyl)ethene dimer

Chemical Property of (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer

There total 2 articles about (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3-hydroxybenzo[b]tellurophene (272-35-5) → (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer (143077-02-5)

Guidance literature:

With n-butyllithium; In hexane; at 20 ℃; for 3h;

Reference yield:

1-Iodo-2-((Z)-2-iodo-vinyl)-benzene (143077-05-8) → (Z)-2-lithio-1-(o-lithiophenyl)ethene dimer (143077-02-5)

Guidance literature:

With n-butyllithium; In hexane;

Reference yield:

(Z)-2-lithio-1-(o-lithiophenyl)ethene dimer (143077-02-5) → 1-Iodo-2-((Z)-2-iodo-vinyl)-benzene (143077-05-8)

Guidance literature:

With dibutyltin chloride; iodine; Multistep reaction;

upstream raw materials:

3-hydroxybenzo[b]tellurophene

1-Iodo-2-((Z)-2-iodo-vinyl)-benzene

Downstream raw materials:

1-Iodo-2-((Z)-2-iodo-vinyl)-benzene

1-methyl-2-[(1Z)-prop-1-en-1-yl]benzene

Refernces