trimethylamine borane

Base Information Edit

Chemical Name:trimethylamine borane
CAS No.:1231953-83-5
Molecular Formula:BH₃*C₃H₉N
Molecular Weight:72.946
Hs Code.:
Mol file:1231953-83-5.mol

Synonyms:trimethylamine borane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trimethylamine borane Edit

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Technology Process of trimethylamine borane

There total 7 articles about trimethylamine borane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: borane pyridine complex

: 75-50-3
trimethylamine

: 110-86-1
pyridine

: 1231953-83-5
trimethylamine borane

Guidance literature:: equil. react.; equimolar mixt. of reactants;
DOI:10.1021/ja01254a031

Reference yield: 45.6%

: 16940-66-2
sodium tetrahydroborate

: 33797-51-2
eschenmoser's salt

: 1231953-83-5
trimethylamine borane

: 7681-82-5,24359-64-6,41927-88-2,115813-40-6
sodium iodide

Guidance literature:: In diethyl ether; React. of starting materials in Et2O (vac. distd., -196°C), warming to 25°C, and stirring overnight.; Distn. of volatile materials into a -196°C U-trap and fractionalcondensation at -68 and -196°C yields Me3N*BH3 in the -68°C trap.;

Reference yield: 45.3%

: 34370-18-8
Li⁽¹⁺⁾*B₅H₈^(1-)=LiB₅H₈

: 33797-51-2
eschenmoser's salt

: 99657-83-7
[(CH₃)2NCH₂]B₅H₈

: 1231953-83-5
trimethylamine borane

: 10377-51-2
lithium iodide

Guidance literature:: In diethyl ether; React. of starting compd. under N2 at -78°C with stirring, slow warming after 1 h to -10°C over a period of 2 h.; Distg. of volatile materials into -63 (white solid) and -196°C (ether, B5H9) U-traps. Further purifn. of solid by fractional condensation (-45°C). Distn. of B5H8-compd. requires several days, because of its low volatility. Elem. anal.;