bromo-phenyl-acetic acid butyl ester

Base Information

• Chemical Name: bromo-phenyl-acetic acid butyl ester
• CAS No.: 56070-50-9
• Molecular Formula: C₁₂H₁₅BrO₂
• Molecular Weight: 271.154
• Mol file: 56070-50-9.mol

Synonyms:bromo-phenyl-acetic acid butyl ester

Chemical Property of bromo-phenyl-acetic acid butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bromo-phenyl-acetic acid butyl ester

There total 3 articles about bromo-phenyl-acetic acid butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

butyl mandelate (14007-02-4,119718-90-0) → bromo-phenyl-acetic acid butyl ester (56070-50-9)

Guidance literature:

With sulfurous dibromide; triethylamine; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1039/c6ra25562k

Reference yield:

MANDELIC ACID (611-71-2,611-72-3,17199-29-0,90-64-2) → bromo-phenyl-acetic acid butyl ester (56070-50-9)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 4 h / 20 °C

2: sulfurous dibromide; triethylamine / dichloromethane / 16 h / 20 °C

With sulfurous dibromide; thionyl chloride; triethylamine; In dichloromethane;

DOI:10.1039/c6ra25562k

Reference yield:

→ bromo-phenyl-acetic acid butyl ester (56070-50-9)

Guidance literature:

/BRN= 2261300/;

DOI:10.1002/ardp.19522850705

upstream raw materials:

butyl mandelate

MANDELIC ACID

Refernces