4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide

Base Information

• Chemical Name: 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide
• CAS No.: 13921-67-0
• Molecular Formula: C₁₄H₁₅N₃O₂
• Molecular Weight: 257.292
• Mol file: 13921-67-0.mol

Synonyms:4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide

Chemical Property of 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide

There total 10 articles about 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline (13921-71-6) → 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide (13921-67-0)

Guidance literature:

With ammonia; water; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; benzene;

Reference yield: 55.0%

methyl yellow (60-11-7) → 4-(phenyl-ONN-azoxy)-N,N-dimethylaniline amino oxide (13921-67-0)

Guidance literature:

With dihydrogen peroxide; In acetic acid; at 40 ℃; for 15h;

Reference yield:

→ N,N-dimethyl-4-((Z)-phenyl-ONN-azoxy)-aniline-N-oxide (13921-67-0)

Guidance literature:

With dihydrogen peroxide; at 40 ℃;

DOI:10.1039/j39670000674 DOI:10.1016/0040-4020(59)80067-3 DOI:10.1021/jo01275a023

upstream raw materials:

4-(phenylazo)-N,N-dimethylaniline amino oxide

methyl yellow

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline

N,N-dimethyl-4-(phenyl-trans-azo)-aniline-N-oxide

Downstream raw materials:

formic acid-(N-methyl-4-phenylazo-anilide)

N-methyl-4-aminoazobenzene

methyl yellow

4-(phenyl-ONN-azoxy)-N,N-dimethylaniline

Refernces

• 1、 Pentimalli, Luciano,Milani, Giovanni. "POSITIONAL ISOMERS OF 4-PHENYLAZO-N,N-DIMETHYLANILINE N-OXIDES". . p. 529 - 532. Retrieved 2007/10/02.