(E)-1-propenyl (Z)-1-propenyl disulfide

Base Information

• Chemical Name: (E)-1-propenyl (Z)-1-propenyl disulfide
• CAS No.: 121609-82-3
• Molecular Formula: C₆H₁₀S₂
• Molecular Weight: 146.277
• Mol file: 121609-82-3.mol

Synonyms:(E)-1-propenyl (Z)-1-propenyl disulfide

Chemical Property of (E)-1-propenyl (Z)-1-propenyl disulfide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (E)-1-propenyl (Z)-1-propenyl disulfide

There total 2 articles about (E)-1-propenyl (Z)-1-propenyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Z)-1-propenyl bromide (590-13-6) → (Z,Z)-bis-(1-propenyl) sulfide (37981-36-5) + (E,Z)-bis-(1-propenyl) sulfide (37981-37-6) + (Z,Z)-bis-(1-propenyl) disulfide (23838-22-4) + 1,2-di-((E)-prop-1-en-1-yl)disulfane (23838-23-5) + (E)-1-propenyl (Z)-1-propenyl disulfide (121609-82-3)

Guidance literature:

With sulfur; In tetrahydrofuran; at 20 ℃; for 1h; Cooling with ice;

DOI:10.1016/j.foodchem.2018.12.112

Reference yield:

1-propenylmagnesium bromide (13154-14-8,13154-15-9,14092-04-7,1730-25-2) → (Z,Z)-bis-(1-propenyl) sulfide (37981-36-5) + (E,Z)-bis-(1-propenyl) sulfide (37981-37-6) + (E,E)-bis-(1-propenyl) sulfide (65819-74-1) + (Z,Z)-bis-(1-propenyl) disulfide (23838-22-4) + 1,2-di-((E)-prop-1-en-1-yl)disulfane (23838-23-5) + (E)-1-propenyl (Z)-1-propenyl disulfide (121609-82-3)

Guidance literature:

With sulfur; In tetrahydrofuran; at 20 ℃; for 1h; Cooling with ice;

DOI:10.1016/j.foodchem.2018.12.112

Reference yield:

(E)-1-propenyl (Z)-1-propenyl disulfide (121609-82-3) → 3,4-dimethylthiophene (632-15-5) + cis-2-Mercapto-3,4-dimethyl-2,3-dihydrothiophene (131425-49-5,131425-50-8,137363-86-1) + trans-2-Mercapto-3,4-dimethyl-2,3-dihydrothiophene (131425-49-5,131425-50-8,137363-86-1)

Guidance literature:

In benzene; at 85 ℃; for 3h; Mechanism; other Bis(1-propenyl) disulfides;

DOI:10.1016/S0040-4039(00)97788-8

upstream raw materials:

(Z)-1-propenyl bromide

1-propenylmagnesium bromide

Downstream raw materials:

3,4-dimethylthiophene

cis-2-Mercapto-3,4-dimethyl-2,3-dihydrothiophene

trans-2-Mercapto-3,4-dimethyl-2,3-dihydrothiophene

Refernces