1,2,3-trihydrotetrafluoropropyl dichlorophosphite

Base Information

• Chemical Name: 1,2,3-trihydrotetrafluoropropyl dichlorophosphite
• CAS No.: 65611-14-5
• Molecular Formula: C₃H₃Cl₂F₄OP
• Molecular Weight: 232.93
• Mol file: 65611-14-5.mol

Synonyms:1,2,3-trihydrotetrafluoropropyl dichlorophosphite

Chemical Property of 1,2,3-trihydrotetrafluoropropyl dichlorophosphite

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 1,2,3-trihydrotetrafluoropropyl dichlorophosphite

There total 1 articles about 1,2,3-trihydrotetrafluoropropyl dichlorophosphite which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

bis(1,1,3-trihydroperfluoropropyl) phosphorochloridite (2241-67-0) → 1,2,3-trihydrotetrafluoropropyl dichlorophosphite (65611-14-5) + tris(2,2,3,3-tetrafluoropropyl)phosphite (2241-68-1)

Guidance literature:

at 20 - 25 ℃; for 840h; Product distribution; object of study - disproportionation;

Reference yield: 85.0%

ethanol (64-17-5) + 1,2,3-trihydrotetrafluoropropyl dichlorophosphite (65611-14-5) → phosphonic acid bis-(2,2,3,3-tetrafluoro-propyl) ester (65611-25-8) + phosphonic acid diethyl ester (762-04-9) + ethyl 1,1,3-trihydroperfluoropropyl phosphite

Guidance literature:

Ambient temperature;

upstream raw materials:

bis(1,1,3-trihydroperfluoropropyl) phosphorochloridite

Downstream raw materials:

phosphonic acid bis-(2,2,3,3-tetrafluoro-propyl) ester

phosphonic acid diethyl ester

Refernces

• 1、 Konovalova, I. V.,Burnaeva, L. A.,Khusnutdinova, E. K.,Khafizova, G. S.,Pudovik, A. N.. "BIS(2,2,3,3-TETRAFLUOROPROPYL) PHOSPHORISOCYANATIDITE AND TRIS(2,2,3,3-TETRAFLUOROPROPYL) PHOSPHITE IN REACTIONS WITH CARBONYL COMPOUNDS". . p. 1943 - 1947. Retrieved 2007/10/02.