3,4'-dibenzoylbiphenyl

Base Information

• Chemical Name: 3,4'-dibenzoylbiphenyl
• CAS No.: 159277-06-2
• Molecular Formula: C₂₆H₁₈O₂
• Molecular Weight: 362.428
• Mol file: 159277-06-2.mol

Synonyms:3,4'-dibenzoylbiphenyl

Chemical Property of 3,4'-dibenzoylbiphenyl

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4'-dibenzoylbiphenyl

There total 2 articles about 3,4'-dibenzoylbiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

biphenyl-3,4′-dicarboxylic acid (92152-01-7) → 3,4'-dibenzoylbiphenyl (159277-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1: SOCl₂ / 5 h / Heating

2: AlCl₃ / 3 h / Heating

With aluminium trichloride; thionyl chloride;

DOI:10.1021/ja00104a033

Reference yield:

Biphenyl-3,4'-dicarbonyl dichloride (149602-72-2) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1) → 3,4'-dibenzoylbiphenyl (159277-06-2)

Guidance literature:

With aluminium trichloride; for 3h; Yield given; Heating;

DOI:10.1021/ja00104a033

Reference yield: 85.0%

3,4'-dibenzoylbiphenyl (159277-06-2) → 3,4'-dibenzoylbiphenyl dihydrazone (159277-05-1)

Guidance literature:

With hydrazine hydrate; In ethanol; for 24h; Heating;

DOI:10.1021/ja00104a033

upstream raw materials:

Biphenyl-3,4'-dicarbonyl dichloride

benzene

biphenyl-3,4′-dicarboxylic acid

Downstream raw materials:

3,4'-dibenzoylbiphenyl dihydrazone

3,4'-bis(phenyldiazomethyl)biphenyl

Refernces