C₅₅H₄₄O₁₃

Base Information

• Chemical Name: C₅₅H₄₄O₁₃
• CAS No.: 244242-29-3
• Molecular Formula: C₅₅H₄₄O₁₃
• Molecular Weight: 912.947
• Mol file: 244242-29-3.mol

Synonyms:C₅₅H₄₄O₁₃

Chemical Property of C₅₅H₄₄O₁₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₅₅H₄₄O₁₃

There total 5 articles about C₅₅H₄₄O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C23H19ClO4 (244242-28-2) + C9H6O5(2-)*2K(1+) → C55H44O13 (244242-29-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; potassium bromide; In N,N-dimethyl-formamide; at 80 ℃;

DOI:10.1021/ol9907724

Reference yield:

C15H24O5Si2 → C55H44O13 (244242-29-3)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃; SOCl₂ / CH₂Cl₂

2: 97 percent / DCC; DPTS / tetrahydrofuran; CH₂Cl₂

3: 81 percent / KBr; DIPEA / dimethylformamide / 80 °C

With thionyl chloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; potassium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol9907724

Reference yield:

5-(chloromethyl)isophthalic acid (244242-23-7) → C55H44O13 (244242-29-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 97 percent / DCC; DPTS / tetrahydrofuran; CH₂Cl₂

2: 81 percent / KBr; DIPEA / dimethylformamide / 80 °C

With N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; 4-(dimethylamino)pyridinium tosylate; potassium bromide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1021/ol9907724

upstream raw materials:

C₂₃H₁₉ClO₄

5-(chloromethyl)isophthalic acid

diethyl 5-(hydroxymethyl)isophthalate

5-(hydroxymethyl)isophthalic acid

Refernces