Technology Process of N-(2-benzamido-1-carboxy-3-phenylpropyl)-Ala-Pro
There total 8 articles about N-(2-benzamido-1-carboxy-3-phenylpropyl)-Ala-Pro which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetic acid / methanol / 72 h
2: 1.) HCl, 2.) di-tert-butyldicarbonate, triethylamine / 1.) RT, 24 h, 2.) methanol, 3 h
3: Amberlyst 15 resin / 240 h / 60 °C
4: triethylamine / CH2Cl2; methanol
5: TFA
6: triethylamine / CH2Cl2
7: 96 percent / aq. NaOH / 24 h
With
hydrogenchloride; sodium hydroxide; Amberlyst 15 resin; di-tert-butyl dicarbonate; acetic acid; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1021/jm00382a008
- Guidance literature:
-
Multi-step reaction with 7 steps
1: acetic acid / methanol / 72 h
2: 1.) HCl, 2.) di-tert-butyldicarbonate, triethylamine / 1.) RT, 24 h, 2.) methanol, 3 h
3: Amberlyst 15 resin / 240 h / 60 °C
4: triethylamine / CH2Cl2; methanol
5: TFA
6: triethylamine / CH2Cl2
7: 96 percent / aq. NaOH / 24 h
With
hydrogenchloride; sodium hydroxide; Amberlyst 15 resin; di-tert-butyl dicarbonate; acetic acid; triethylamine; trifluoroacetic acid;
In
methanol; dichloromethane;
DOI:10.1021/jm00382a008
