(1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene

Base Information Edit

Chemical Name:(1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene
CAS No.:5263-68-3
Molecular Formula:C₉H₁₃N
Molecular Weight:135.209
Hs Code.:2933990090
Mol file:5263-68-3.mol

Synonyms:4,7-Methanoisoindoline,3a,4,7,7a-tetrahydro- (6CI,8CI); 2-Azadicyclopentadiene, 2,3-dihydro-;4,7-Endomethylene-4,7,8,9-tetrahydroisoindoline; NSC 31983

Suppliers and Price of (1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
500mg
$ 150.00

Crysdot
(3AR,4S,7R,7aS)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methanoisoindole 95+%
5g
$ 752.00

Chemenu
(3AR,4S,7R,7aS)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methanoisoindole 95%
5g
$ 711.00

Biosynth Carbosynth
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
1 g
$ 255.00

Biosynth Carbosynth
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
2 g
$ 434.00

Biosynth Carbosynth
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
500 mg
$ 150.00

Biosynth Carbosynth
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
250 mg
$ 85.00

Biosynth Carbosynth
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
5 g
$ 868.00

Alichem
(3AR,4S,7R,7aS)-2,3,3a,4,7,7a-hexahydro-1H-4,7-methanoisoindole
5g
$ 813.20

AK Scientific
(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene
1g
$ 394.00

Total 14 raw suppliers

Chemical Property of (1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene Edit

Chemical Property:

Vapor Pressure:3.5E-09mmHg at 25°C
Boiling Point:205.3°Cat760mmHg
Flash Point:77.5°C
PSA：12.03000
Density:1.049g/cm³
LogP:1.35670

Purity/Quality:

98%min ^*data from raw suppliers

(1R,2S,6R,7S)-4-Azatricyclo[5.2.1.0~2,6~]dec-8-ene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene

There total 6 articles about (1R,2S,6R,7S)-4-azatricyclo[5.2.1.0~2,6~]dec-8-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 6265-30-1
(1R,2S,6R,7S)-4-azatricyclo[5.2.1.0(2,6)]dec-8-ene-3,5-dione

: 5263-68-3,40594-05-6
(1α,2α,6α,7α)-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: With lithium aluminium tetrahydride; In diethylene glycol dimethyl ether; 1) 45 deg C, 1h; 2) 120-130 deg C, 2 h; 3) 110-120 deg C, 4 h;
DOI:10.1007/BF00505988

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 5263-68-3,40594-05-6
(1α,2α,6α,7α)-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / benzene / 12 h / 6 °C

2: 71 percent / urea / 1 h / 170 - 180 °C

3: 98 percent / LiAlH₄ / bis-(2-methoxy-ethyl) ether / 1) 45 deg C, 1h; 2) 120-130 deg C, 2 h; 3) 110-120 deg C, 4 h

With lithium aluminium tetrahydride; urea; In diethylene glycol dimethyl ether; benzene;
DOI:10.1007/BF00505988

Reference yield:

: 129-64-6
3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

: 5263-68-3,40594-05-6
(1α,2α,6α,7α)-4-azatricyclo[5.2.1.0^2,6]dec-8-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NH₄OH, 2.) Ac₂O / 2.) reflux, 2 h

2: LAH / tetrahydrofuran

With ammonium hydroxide; lithium aluminium tetrahydride; acetic anhydride; In tetrahydrofuran;