Technology Process of (4S)-4-isopropyl-2-phenyl-4,5-dihydro-1λ6,3-thiazole 1,1-dioxide
There total 5 articles about (4S)-4-isopropyl-2-phenyl-4,5-dihydro-1λ6,3-thiazole 1,1-dioxide which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium permanganate; N-benzyl-N,N,N-triethylammonium chloride; benzoic acid;
In
dichloromethane;
for 15h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 48 percent / NEt3 / CH2Cl2 / 20 h / Ambient temperature
2: 85 percent / P2S5 / CH2Cl2 / 40 h / Heating
3: 85 percent / PhCO2H, aq. KMnO4, benzyltriethylammonium chloride / CH2Cl2 / 15 h / Ambient temperature
With
potassium permanganate; tetraphosphorus decasulfide; N-benzyl-N,N,N-triethylammonium chloride; triethylamine; benzoic acid;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 48 percent / NEt3 / CH2Cl2 / 20 h / Ambient temperature
2: 85 percent / P2S5 / CH2Cl2 / 40 h / Heating
3: 85 percent / PhCO2H, aq. KMnO4, benzyltriethylammonium chloride / CH2Cl2 / 15 h / Ambient temperature
With
potassium permanganate; tetraphosphorus decasulfide; N-benzyl-N,N,N-triethylammonium chloride; triethylamine; benzoic acid;
In
dichloromethane;