W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅

Base Information

• Chemical Name: W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅
• CAS No.: 90968-01-7
• Molecular Formula: C₂₆H₂₀NO₂PS₂W
• Molecular Weight: 657.406
• Mol file: 90968-01-7.mol

Synonyms:W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅

Chemical Property of W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅

There total 1 articles about W(CO)2(C₅H₅)(C₆H₅)2P(S)C(S)NC₆H₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

tricarbonylcyclopentadienyltungsten(II) chloride + (C6H5)2P(S)C(S)NHC6H5 (7067-81-4) → W(CO)2(C5H5)(C6H5)2P(S)C(S)NC6H5 (90968-01-7)

Guidance literature:

With KOH; In ethanol; keeping soln. of W-complex, ligand and KOH for a few hours at 25°C under N2; evapn. to dryness; chromy. (silica column, CH2Cl2/n-hexane); elem. anal.;

Reference yield: 35.0%

W(CO)2(C5H5)(C6H5)2P(S)C(S)NC6H5 (90968-01-7) → W(CO)2(C5H5)(SP(C6H5)2) (76374-51-1)

Guidance literature:

In not given; byproducts: C6H5NCS; refluxing under N2;

upstream raw materials:

(C₆H₅)2P(S)C(S)NHC₆H₅

Downstream raw materials:

W(CO)2(C₅H₅)(SP(C₆H₅)2)

Refernces