C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH

Base Information

• Chemical Name: C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH
• CAS No.: 865835-76-3
• Molecular Formula: C₁₅H₂₈B₁₀O₃
• Molecular Weight: 364.496
• Mol file: 865835-76-3.mol

Synonyms:C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH

Chemical Property of C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH

Chemical Property:

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Technology Process of C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH

There total 1 articles about C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂COOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

C6H5CH2OCH2CH2CH2CB10H10CCH2CH2CH2OH (865835-75-2) + [bis(acetoxy)iodo]benzene (3240-34-4) → C6H5CH2OCH2CH2CH2CB10H10CCH2CH2COOH (865835-76-3)

Guidance literature:

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; In not given;

DOI:10.1021/ja053730l

Reference yield: 99.0%

Pentaerythritol (115-77-5) + C6H5CH2OCH2CH2CH2CB10H10CCH2CH2COOH (865835-76-3) → (C6H5CH2OCH2CH2CH2CB10H10CCH2CH2COOCH2)4C

Guidance literature:

With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; 4-(dimethylamino)pyridinium tosylate; In pyridine; dichloromethane; CH2Cl2-pyridine 3:2, room temp., > 12 h; column chromy.;

DOI:10.1021/ja053730l

upstream raw materials:

C₆H₅CH₂OCH₂CH₂CH₂CB₁₀H₁₀CCH₂CH₂CH₂OH

[bis(acetoxy)iodo]benzene

Refernces