N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide

Base Information

• Chemical Name: N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide
• CAS No.: 96134-80-4
• Molecular Formula: C11H17 N3 O3 S
• Molecular Weight: 271.34
• Hs Code.: 2935009090
• DSSTox Substance ID: DTXSID30351092
• Wikidata: Q82127222
• Mol file: 96134-80-4.mol

Synonyms:96134-80-4;N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide;N,N-diethyl-3-(hydrazinecarbonyl)benzenesulfonamide;n,n-diethyl-3-hydrazinocarbonyl-benzenesulfonamide;TimTec1_000839;Oprea1_100015;DTXSID30351092;HMS1536G03;MFCD01197380;AKOS000116265;NCGC00175068-01;EN300-03575;SR-01000028602;Benzoic acid,3-[(diethylamino)sulfonyl]-,hydrazide;N,N-diethyl-3-(hydrazinocarbonyl)benzenesulfonamide;SR-01000028602-1;BRD-K74268134-001-01-6;Z56785834;F8881-5316;N,N-Diethyl-3-(hydrazinecarbonyl)-benzene-1-sulfonamide;BENZOIC ACID,3-[(DIETHYLAMINO)SULFONYL]-, HYDRAZIDE

Chemical Property of N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 104.37000
• Density: 1.259g/cm³
• LogP: 2.67650
• XLogP3: 0.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 5
• Exact Mass: 271.09906259
• Heavy Atom Count: 18
• Complexity: 374

Purity/Quality:

98%Min ^*data from raw suppliers

N,N-Diethyl-3-(hydrazinecarbonyl)-benzene-1-sulfonamide 95%+ ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCN(CC)S(=O)(=O)C1=CC=CC(=C1)C(=O)NN

Technology Process of N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide

There total 4 articles about N,N-diethyl-3-(hydrazinecarbonyl)benzene-1-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C12H17NO4S (445298-39-5) → 3-<(Diethylamino)sulfonyl>benzoic Acid Hydrazide (96134-80-4)

Guidance literature:

With hydrazine; In methanol; at 130 ℃; for 0.5h; Microwave irradiation;

DOI:10.1016/j.bmcl.2015.06.054

Reference yield:

3-Carboxybenzenesulfonyl chloride (4025-64-3) → 3-<(Diethylamino)sulfonyl>benzoic Acid Hydrazide (96134-80-4)

Guidance literature:

Multi-step reaction with 3 steps

1: H₂O

2: HCl gas / Heating

3: hydrazine hydrate / Heating

With hydrogenchloride; hydrazine hydrate; In water;

Reference yield:

<(Diethylamino)sulfonyl>benzoic Acid (1576-46-1) → 3-<(Diethylamino)sulfonyl>benzoic Acid Hydrazide (96134-80-4)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl gas / Heating

2: hydrazine hydrate / Heating

With hydrogenchloride; hydrazine hydrate;

upstream raw materials:

3-Carboxybenzenesulfonyl chloride

<(Diethylamino)sulfonyl>benzoic Acid

C₁₂H₁₇NO₄S

Downstream raw materials:

N,N-Diethyl-3-(5-phenyl-[1,3,4]oxadiazol-2-yl)-benzenesulfonamide

N,N-Diethyl-3-[1,3,4]oxadiazol-2-yl-benzenesulfonamide

N,N-Diethyl-3-(5-methyl-[1,3,4]oxadiazol-2-yl)-benzenesulfonamide

Refernces

• 1、 Peet, Norton P.,Sunder, Shyam. "Factors Which Influence the Formation of Oxadiazoles from Anthranilhydrazides and Other Benzoylhydrazines". . p. 1807 - 1816. Retrieved 2007/10/02.