[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester

Base Information

• Chemical Name: [6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester
• CAS No.: 928118-30-3
• Molecular Formula: C₂₁H₃₅NO₃
• Molecular Weight: 349.514
• Mol file: 928118-30-3.mol

Synonyms:[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester

Chemical Property of [6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of [6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester

There total 1 articles about [6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) + 1-azido-6-(4-phenylbutoxy)hexane (168412-89-3) → [6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester (928118-30-3)

Guidance literature:

1-azido-6-(4-phenylbutoxy)hexane; With hydrogen; palladium catalyst;

di-tert-butyl dicarbonate;

Reference yield: 84.0%

[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester (928118-30-3) → D 2543 (97664-58-9)

Guidance literature:

[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1.5h;

With ammonia; In dichloromethane; pH=10 - 11;

Reference yield:

[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester (928118-30-3) + 5-(2-bromoacetyl)-2-hydroxybenzaldehyde (115787-50-3) → [2-(3-formyl-4-hydroxyphenyl)-2-oxoethyl]-[6-(4-phenylbutoxy)hexyl]carbamic acid tert-butyl ester (1056135-44-4)

Guidance literature:

[6-(4-phenylbutoxy)hexyl]carbamic acid ter-butyl ester; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h;

5-(2-bromoacetyl)-2-hydroxybenzaldehyde; In tetrahydrofuran; at 5 - 20 ℃;

upstream raw materials:

di-tert-butyl dicarbonate

1-azido-6-(4-phenylbutoxy)hexane

Downstream raw materials:

D 2543

[2-(3-formyl-4-hydroxyphenyl)-2-oxoethyl]-[6-(4-phenylbutoxy)hexyl]carbamic acid tert-butyl ester

Refernces