1,3,6,8-Tetranitrocarbazole

Base Information

• Chemical Name: 1,3,6,8-Tetranitrocarbazole
• CAS No.: 4543-33-3
• Molecular Formula: C12H5 N5 O8
• Molecular Weight: 347.2
• Hs Code.: 2933990090
• European Community (EC) Number: 224-898-0
• NSC Number: 15106
• UNII: 6M5VL5EW3V
• DSSTox Substance ID: DTXSID1063516
• Nikkaji Number: J235.991J
• Wikidata: Q2806556
• Mol file: 4543-33-3.mol

Synonyms:1,3,6,8-Tetranitrocarbazole;4543-33-3;Nirosan;1,3,6,8-Tetranitro-9H-carbazole;9H-Carbazole, 1,3,6,8-tetranitro-;Carbazole, 1,3,6,8-tetranitro-;EINECS 224-898-0;NSC 15106;1,3,6,8-Tetranitrokarbazol [Czech];BRN 0363292;6M5VL5EW3V;1,3,6,8-Tetranitrokarbazol;AI3-14491;NSC-15106;5-20-08-00056 (Beilstein Handbook Reference);UNII-6M5VL5EW3V;1,6,8-Tetranitrocarbazole;SCHEMBL56979;Carbazole,3,6,8-tetranitro-;DTXSID1063516;C12H5N5O8;9H-Carbazole,3,6,8-tetranitro-;NSC15106;C12-H5-N5-O8;1,3,6,8-Tetranitro-9H-carbazole #;LS-51846;CS-0452627;FT-0606537;T0159;Q2806556;1,3,6,8-Tetranitrocarbazole (wetted with ca. 40% Water) (unit weight on dry weight basis)

Chemical Property of 1,3,6,8-Tetranitrocarbazole

Chemical Property:

• Vapor Pressure: 4.34E-16mmHg at 25°C
• Melting Point: 291 °C
• Refractive Index: 1.7000 (estimate)
• Boiling Point: 650.5°C at 760 mmHg
• Flash Point: 347.2°C
• PSA: 199.07000
• Density: 1.893g/cm³
• LogP: 5.04670
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 8
• Rotatable Bond Count: 0
• Exact Mass: 347.01381213
• Heavy Atom Count: 25
• Complexity: 555

Purity/Quality:

98%,99%, ^*data from raw suppliers

1,3,6,8-Tetranitrocarbazole (wetted with ca. 40% Water) (unit weight on dry weight basis) >70.0%(HPLC) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=C(C=C(C2=C1C3=C(N2)C(=CC(=C3)[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-])[N+](=O)[O-]

Technology Process of 1,3,6,8-Tetranitrocarbazole

There total 11 articles about 1,3,6,8-Tetranitrocarbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2'-Dimethoxy-3,5,3',5'-tetranitro-biphenyl (67651-42-7) → 1,3,6,8-tetranitrocarbazole (4543-33-3)

Guidance literature:

With ethanol; ammonia; at 140 - 150 ℃;

Reference yield:

9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 1,3,6,8-tetranitrocarbazole (4543-33-3)

Guidance literature:

With nitric acid;

Reference yield:

ethyl nitrate (625-58-1) + 9H-carbazole (86-74-8,105184-46-1,97960-57-1) → 1,3,6,8-tetranitrocarbazole (4543-33-3)

Guidance literature:

With sulfuric acid; at 0 ℃;

upstream raw materials:

2,2'-Dimethoxy-3,5,3',5'-tetranitro-biphenyl

9H-carbazole

sulfuric acid

water

Downstream raw materials:

1,3,6,8-tetrachlorocarbazole