N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Base Information Edit

Chemical Name:N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide
CAS No.:1338351-00-0
Molecular Formula:C₂₁H₂₄N₂O₂S
Molecular Weight:368.5
Hs Code.:
Mol file:1338351-00-0.mol

Synonyms:N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide Edit

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Technology Process of N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

There total 7 articles about N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 69174-69-2
5-isopropyl-3,8-dimethyl-azulene-1-sulfonyl chloride

: 106-50-3
1,4-phenylenediamine

: 1338351-00-0
N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Guidance literature:: With pyridine; triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2011.08.018

Reference yield:

: C₂₆H₃₂N₂O₄S

: 1338351-00-0
N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 3h;

Reference yield:

: 6223-35-4
Azulon

: 1338351-00-0
N-(4-aminophenyl)-3,8-dimethyl-5-isopropyl-1-azulene sulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 0.17 h / Cooling with ice

2: pyridine; triethylamine / dichloromethane / 1 h / 20 °C

With pyridine; oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane;
DOI:10.1016/j.bmcl.2011.08.018