Technology Process of Mo(C5H5)(CO)(NO)(CH2CHCH2Sn(C6H5)3)
There total 3 articles about Mo(C5H5)(CO)(NO)(CH2CHCH2Sn(C6H5)3) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
To a soln. of complex in THF at -78°C was added allyl iodide, the mixt. was allowed to warm slowly to room temp. (N2 atm.);; the solvent was pumped off, ppt. was dissolved in toluene, filtered, chromd. on silica gel with hexane:toluene=1:1, concd., hexane was added, standing at -20°C; elem. anal.;;
- Guidance literature:
-
In
toluene;
Irradiation (UV/VIS); Reflux in toluene or irradiation with a 100-W Hanovia lamp for 3 h;;
- Guidance literature:
-
In
tetrahydrofuran;
To a soln. of complex in THF at -78°C was added allyl bromide, the mixt. was allowed to warm slowly to room temp. (N2 atm.);; the solvent was pumped off, ppt. was dissolved in toluene, filtered, chromd. on silica gel with hexane:toluene=1:1, concd., hexane was added, standing at -20°C; elem. anal.;;
