Technology Process of Sarcolysin
There total 12 articles about Sarcolysin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 70 percent / H2 / Raney Ni / methanol / 40 °C / 3361.5 Torr
2: 1.) POCl3, 2.) conc. HCl / 1.) benzene, reflux, 15 min, 2.) reflux, 4 h
With
hydrogenchloride; hydrogen; trichlorophosphate;
nickel;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 52 percent / methanol / 0.33 h / Heating
2: 70 percent / H2 / Raney Ni / methanol / 40 °C / 3361.5 Torr
3: 1.) POCl3, 2.) conc. HCl / 1.) benzene, reflux, 15 min, 2.) reflux, 4 h
With
hydrogenchloride; hydrogen; trichlorophosphate;
nickel;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 56 percent / pyridine / 24 h / Ambient temperature
2: 52 percent / methanol / 0.33 h / Heating
3: 70 percent / H2 / Raney Ni / methanol / 40 °C / 3361.5 Torr
4: 1.) POCl3, 2.) conc. HCl / 1.) benzene, reflux, 15 min, 2.) reflux, 4 h
With
hydrogenchloride; hydrogen; trichlorophosphate;
nickel;
In
pyridine; methanol;
