Acetyl chloride 4-nitrophenylhydrazone

Base Information

• Chemical Name: Acetyl chloride 4-nitrophenylhydrazone
• CAS No.: 39209-25-1
• Molecular Formula: C8H8ClN3O2
• Molecular Weight: 213.62102
• Nikkaji Number: J90.806A
• Mol file: 39209-25-1.mol

Synonyms:Acetyl chloride 4-nitrophenylhydrazone;ACETYL CHLORIDE, p-NITROPHENYLHYDRAZONE;39209-25-1;1-Chloroethanone p-nitrophenyl hydrazone

Chemical Property of Acetyl chloride 4-nitrophenylhydrazone

Chemical Property:

• Vapor Pressure: 0.000134mmHg at 25°C
• Boiling Point: 333.7°C at 760 mmHg
• Flash Point: 155.6°C
• PSA: 70.21000
• Density: 1.36g/cm³
• LogP: 3.17510
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 213.0305042
• Heavy Atom Count: 14
• Complexity: 231

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=NNC1=CC=C(C=C1)[N+](=O)[O-])Cl
• Isomeric SMILES: C/C(=N\NC1=CC=C(C=C1)[N+](=O)[O-])/Cl

Technology Process of Acetyl chloride 4-nitrophenylhydrazone

There total 1 articles about Acetyl chloride 4-nitrophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ N-p-nitrophenylethanehydrazonoyl chloride (39209-25-1)

Guidance literature:

/BRN= 1842183/;

Reference yield: 80.0%

N-p-nitrophenylethanehydrazonoyl chloride (39209-25-1) + 1,3-dimethyl-8-chloroxanthine (85-18-7) → 1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine (348086-41-9)

Guidance literature:

With triethylamine; In 1,4-dioxane; Heating;

DOI:10.1021/jo001626a

Reference yield: 77.0%

N-p-nitrophenylethanehydrazonoyl chloride (39209-25-1) + Potassium; 2-chloro-3,5-dinitro-benzoate → 2-Chloro-3,5-dinitro-benzoic acid N'-acetyl-N-(4-nitro-phenyl)-hydrazide

Guidance literature:

In 1,4-dioxane; for 30h; Heating;

DOI:10.1007/BF00866599

Downstream raw materials:

C₁₂H₁₃N₅O₂S

1-(4-nitrophenyl)-3-methyl-5-(thiazol-4-yl)-1,2,4-triazole

1,3-dimethyl-2,4-dioxo-6-methyl-8-(p-nitrophenyl)-1,2,3,4-tetrahydro[1,2,4]triazolo[3,4-f]purine