4-Acetoxy-3,5-di-tert-butylbenzaldehyde

Base Information

• Chemical Name: 4-Acetoxy-3,5-di-tert-butylbenzaldehyde
• CAS No.: 87133-21-9
• Molecular Formula: C₁₇H₂₄O₃
• Molecular Weight: 276.376
• Mol file: 87133-21-9.mol

Synonyms:4-Acetoxy-3,5-di-tert-butylbenzaldehyde

Chemical Property of 4-Acetoxy-3,5-di-tert-butylbenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Acetoxy-3,5-di-tert-butylbenzaldehyde

There total 4 articles about 4-Acetoxy-3,5-di-tert-butylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.4%

3-(1,1-Dimethylethyl)-4-hydroxy-benzaldehyde (65678-11-7) → 4-Acetoxy-3,5-di-tert-butylbenzaldehyde (87133-21-9)

Guidance literature:

With hydrogenchloride; perchloric acid; acetic anhydride; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; ethanol; water;

Reference yield: 99.4%

acetic anhydride (108-24-7) + 3,5-di-t-butyl-4-hydroxybenzaldehyde (1620-98-0) → 4-Acetoxy-3,5-di-tert-butylbenzaldehyde (87133-21-9)

Guidance literature:

perchloric acid;

Reference yield: 98.0%

α,α,4-triacetoxy-3,5-di-tert-butyltoluene (859793-58-1) → 4-Acetoxy-3,5-di-tert-butylbenzaldehyde (87133-21-9)

Guidance literature:

With hydrogenchloride; ethanol; water; for 0.166667h; Heating;

upstream raw materials:

2,6-di-tert-butyl-4-methyl-phenol

acetic anhydride

acetic acid

α,α,4-triacetoxy-3,5-di-tert-butyltoluene

Downstream raw materials:

α-(4-acetoxy-3,5-di-tert-butylphenyl)-N-1-hydroxy-2-methylprop-2-ylnitrone

Refernces

• 1、 -. "3,4,5-trisubstituted aryl nitrone compounds, pharmaceutical compositions containing the same and methods for treating inflammation". Page column 17-18. . Retrieved 2008/06/13.
• 2、 Melezhik, A. V.,Vovk, D. N.,Pokhodenko, V. D.. "SPECTRAL PROPERTIES OF FREE-RADICAL DERIVATIVES OF TETRA(4-HYDROXY-3,5-DI-tert-BUTYLPHENYL)PORPHINE". . p. 1442 - 1447. Retrieved 2007/10/02.