Technology Process of C36H28BrN5O7
There total 6 articles about C36H28BrN5O7 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
4-amino-6-bromo-5-cyanopyrrolo[2,3-d]pyrimidine;
With
ammonium sulfate; 1,1,1,3,3,3-hexamethyl-disilazane;
In
m-xylene;
Heating;
1-O-acetyl-5(R)-C-allyl-2,3,5-tri-O-benzoyl-D-ribofuranose;
With
trimethylsilyl trifluoromethanesulfonate;
In
1,2-dichloro-ethane;
for 72h;
Heating;
DOI:10.1016/S0968-0896(00)00221-2
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 6.26 g / pyridine / 20 °C
2.1: CF3COOH / H2O / 1.5 h / 0 °C
3.1: 5.30 g / pyridine / 20 °C
4.1: 2.82 g / aq. H2SO4 / acetic acid / 20 °C
5.1: HMDS; ammonium sulfate / m-xylene / Heating
5.2: 66 percent / TMSOTf / 1,2-dichloro-ethane / 72 h / Heating
With
ammonium sulfate; sulfuric acid; 1,1,1,3,3,3-hexamethyl-disilazane; trifluoroacetic acid;
In
pyridine; water; acetic acid; m-xylene;
5.2: Vorbrueggen condensation;
DOI:10.1016/S0968-0896(00)00221-2
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 6.26 g / pyridine / 20 °C
2.1: CF3COOH / H2O / 1.5 h / 0 °C
3.1: 5.30 g / pyridine / 20 °C
4.1: 2.82 g / aq. H2SO4 / acetic acid / 20 °C
5.1: HMDS; ammonium sulfate / m-xylene / Heating
5.2: 66 percent / TMSOTf / 1,2-dichloro-ethane / 72 h / Heating
With
ammonium sulfate; sulfuric acid; 1,1,1,3,3,3-hexamethyl-disilazane; trifluoroacetic acid;
In
pyridine; water; acetic acid; m-xylene;
5.2: Vorbrueggen condensation;
DOI:10.1016/S0968-0896(00)00221-2