Technology Process of styelsamine-N14-benzamide
There total 7 articles about styelsamine-N14-benzamide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
N-(3,4-dihydroxyphenethyl)benzamide; Kynuramine dihydrobromide;
With
cerium(III) chloride heptahydrate; silver(l) oxide;
In
methanol; acetic acid;
at 40 ℃;
for 1.5h;
Inert atmosphere;
With
hydrogenchloride;
In
water;
at 90 ℃;
for 0.5h;
DOI:10.3390/md11020274
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: boron tribromide / dichloromethane / 20 h / 0 - 20 °C
2.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere
2.2: 0.5 h / 90 °C
With
cerium(III) chloride heptahydrate; boron tribromide; silver(l) oxide;
In
methanol; dichloromethane; acetic acid;
DOI:10.3390/md11020274
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water; ethyl acetate / 0.5 h / 20 °C / Inert atmosphere
2.1: ozone / Cooling with ice
2.2: 1.5 h / 40 °C
3.1: hydrogen bromide / acetic acid / 18 h / 80 °C / Inert atmosphere
4.1: cerium(III) chloride heptahydrate; silver(l) oxide / acetic acid; methanol / 1.5 h / 40 °C / Inert atmosphere
4.2: 0.5 h / 90 °C
With
cerium(III) chloride heptahydrate; hydrogen bromide; ozone; sodium hydroxide; silver(l) oxide;
In
methanol; water; acetic acid; ethyl acetate;
DOI:10.3390/md11020274
