benzyl 4-methoxyphenethylcarbamate

Base Information

• Chemical Name: benzyl 4-methoxyphenethylcarbamate
• CAS No.: 198756-72-8
• Molecular Formula: C₁₇H₁₉NO₃
• Molecular Weight: 285.343
• Mol file: 198756-72-8.mol

Synonyms:benzyl 4-methoxyphenethylcarbamate

Chemical Property of benzyl 4-methoxyphenethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of benzyl 4-methoxyphenethylcarbamate

There total 4 articles about benzyl 4-methoxyphenethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

5-propyl-benzo[1,3]dioxol-2-one + 4-Methoxyphenethylamine (55-81-2) + benzyl alcohol (100-51-6,185532-71-2) → benzyl 4-methoxyphenethylcarbamate (198756-72-8)

Guidance literature:

5-propyl-benzo[1,3]dioxol-2-one; benzyl alcohol; With zinc(II) acetate dihydrate; at 50 ℃; for 16h; Sealed tube;

4-Methoxyphenethylamine; In 2-methyltetrahydrofuran; at 25 ℃; for 16h; Sealed tube;

DOI:10.1002/cssc.201900406

Reference yield: 85.0%

carbon dioxide (124-38-9,18923-20-1) + benzyl chloride (100-44-7) + 4-Methoxyphenethylamine (55-81-2) → benzyl 4-methoxyphenethylcarbamate (198756-72-8)

Guidance literature:

carbon dioxide; 4-Methoxyphenethylamine; With tetra-(n-butyl)ammonium iodide; caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 1h;

benzyl chloride; In N,N-dimethyl-formamide; at 23 ℃; for 5h;

DOI:10.1016/S0040-4020(02)00286-7

Reference yield: 80.0%

benzyl (2-(trifluoro-λ4-boraneyl)ethyl)carbamate, potassium salt + 1-bromo-4-methoxy-benzene (104-92-7) → benzyl 4-methoxyphenethylcarbamate (198756-72-8)

Guidance literature:

With caesium carbonate; palladium diacetate; In water; toluene; at 95 ℃; for 12h;

DOI:10.1021/jo7015955

upstream raw materials:

carbon dioxide

benzyl chloride

4-Methoxyphenethylamine

1-bromo-4-methoxy-benzene

Downstream raw materials:

4-Methoxyphenethylamine

Refernces

• 1、 -. "INHIBITION OF BACTERIAL BIOFILMS WITH ARYL CARBAMATES". Page/Page column 33. . Retrieved 2012/02/01.
• 2、 Salvatore, Ralph N,Chu, Feixia,Nagle, Advait S,Kapxhiu, Elona A,Cross, Richard M,Jung, Kyung Woon. "Efficient Cs2CO3-promoted solution and solid phase synthesis of carbonates and carbamates in the presence of TBAI". . p. 3329 - 3347. Retrieved 2007/10/03.