11H-Dibenzo[c,f][1,2]diazepine

Base Information

• Chemical Name: 11H-Dibenzo[c,f][1,2]diazepine
• CAS No.: 256-91-7
• Molecular Formula: C13H10 N2
• Molecular Weight: 194.236
• Hs Code.: 2933990090
• Mol file: 256-91-7.mol

Synonyms:2,3:6,7-Dibenzo-4,5-diazacyclohepta-2,4,6-triene

Chemical Property of 11H-Dibenzo[c,f][1,2]diazepine

Chemical Property:

• Vapor Pressure: 0.000154mmHg at 25°C
• Boiling Point: 342°C at 760 mmHg
• Flash Point: 152.8°C
• PSA: 24.72000
• Density: 1.17g/cm³
• LogP: 2.87740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 11H-Dibenzo[c,f][1,2]diazepine

There total 1 articles about 11H-Dibenzo[c,f][1,2]diazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-dihydrodibenzo--diazepine (2225-56-1) → 2,2'-methylenedianiline (6582-52-1) + 11H-dibenzo{c,f}-{1,2}diazepine (256-91-7)

Guidance literature:

With hydrogenchloride;

DOI:10.1016/S0040-4039(01)99991-5

Reference yield:

11H-dibenzo{c,f}-{1,2}diazepine (256-91-7) → 2,2'-methylenedianiline (6582-52-1)

Guidance literature:

Multi-step reaction with 2 steps

1: aqueous ethanol; zinc-powder; aqueous NH₃

2: aqueous HCl

With hydrogenchloride; ammonium hydroxide; ethanol; zinc;

DOI:10.1016/S0040-4039(01)99991-5

upstream raw materials:

1,2-dihydrodibenzo--diazepine

Downstream raw materials:

2,2'-methylenedianiline