Technology Process of 2-ethoxycarbonyl-6-isopropylphenol
There total 3 articles about 2-ethoxycarbonyl-6-isopropylphenol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sulfuric acid;
at 20 ℃;
Reflux;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
1.2: 4.33 h / 20 °C / Reflux
1.3: 20 °C
2.1: silver nitrate; sodium hydroxide / ethanol / 20 °C
2.2: 10 - 15 °C / pH 2
3.1: sulfuric acid / 20 °C / Reflux
With
sulfuric acid; silver nitrate; triethylamine; sodium hydroxide; magnesium chloride;
In
tetrahydrofuran; ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: water; lithium hydroxide / tetrahydrofuran / 20 °C
2.1: triethylamine; magnesium chloride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
2.2: 4.33 h / 20 °C / Reflux
2.3: 20 °C
3.1: silver nitrate; sodium hydroxide / ethanol / 20 °C
3.2: 10 - 15 °C / pH 2
4.1: sulfuric acid / 20 °C / Reflux
With
sulfuric acid; water; silver nitrate; triethylamine; sodium hydroxide; magnesium chloride; lithium hydroxide;
In
tetrahydrofuran; ethanol;
