14-bromo-1-phenyl-tetradec-1-yne

Base Information Edit

Chemical Name:14-bromo-1-phenyl-tetradec-1-yne
CAS No.:104827-27-2
Molecular Formula:C₂₀H₂₉Br
Molecular Weight:349.354
Hs Code.:
Mol file:104827-27-2.mol

Synonyms:14-bromo-1-phenyl-tetradec-1-yne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 14-bromo-1-phenyl-tetradec-1-yne Edit

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 14-bromo-1-phenyl-tetradec-1-yne

There total 1 articles about 14-bromo-1-phenyl-tetradec-1-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3344-70-5
1,12-dibromododecane

: 536-74-3
phenylacetylene

: 104827-27-2
14-bromo-1-phenyl-tetradec-1-yne

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; 1.) THF, hexane, 10 deg C, HMPT, 1 h; 2.) THF, 20-25 deg C;

Reference yield:

: 104827-27-2
14-bromo-1-phenyl-tetradec-1-yne

: 40228-93-1
ω-phenyl pentadecanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / PtO₂ / ethyl acetate / 15 h

2: 94 percent / tributylamine / 2 h / Heating

3: 91 percent / 10 N NaOH / Heating

With sodium hydroxide; tributyl-amine; hydrogen; platinum(IV) oxide; In ethyl acetate;