S-(2-iodophenethyl) 4-azidobutanethioate

Base Information

• Chemical Name: S-(2-iodophenethyl) 4-azidobutanethioate
• CAS No.: 461383-65-3
• Molecular Formula: C₁₂H₁₄IN₃OS
• Molecular Weight: 375.233
• Mol file: 461383-65-3.mol

Synonyms:S-(2-iodophenethyl) 4-azidobutanethioate

Chemical Property of S-(2-iodophenethyl) 4-azidobutanethioate

Chemical Property:

Purity/Quality:

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Technology Process of S-(2-iodophenethyl) 4-azidobutanethioate

There total 1 articles about S-(2-iodophenethyl) 4-azidobutanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

4-azidobutanoyl chloride (14468-88-3) + 2-(2-iodophenyl)-1-ethanethiol (177748-62-8) → S-(2-iodophenethyl) 4-azidobutanethioate (461383-65-3)

Guidance literature:

DOI:10.1021/ol026366t

Reference yield: 83.0%

S-(2-iodophenethyl) 4-azidobutanethioate (461383-65-3) → 4-azido-thiobutyric acid S-phenethyl ester + 2-pyrrolidinon (616-45-5) + 2,3-dihydrobenzo(b)thiophene (4565-32-6)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; Heating;

DOI:10.1021/ol026366t

upstream raw materials:

4-azidobutanoyl chloride

2-(2-iodophenyl)-1-ethanethiol

Downstream raw materials:

2-pyrrolidinon

2,3-dihydrobenzo(b)thiophene

Refernces