4-allyl-2,6-dimethoxyphenyl bromoacetate

Base Information

• Chemical Name: 4-allyl-2,6-dimethoxyphenyl bromoacetate
• CAS No.: 691860-36-3
• Molecular Formula: C₁₃H₁₅BrO₄
• Molecular Weight: 315.164
• Mol file: 691860-36-3.mol

Synonyms:4-allyl-2,6-dimethoxyphenyl bromoacetate

Chemical Property of 4-allyl-2,6-dimethoxyphenyl bromoacetate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-allyl-2,6-dimethoxyphenyl bromoacetate

There total 1 articles about 4-allyl-2,6-dimethoxyphenyl bromoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-bromoacetyl chloride (22118-09-8) + 4-allyl-2,6-dimethoxyphenol (6627-88-9) → 4-allyl-2,6-dimethoxyphenyl bromoacetate (691860-36-3)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 0.833333h;

Reference yield:

4-allyl-2,6-dimethoxyphenyl bromoacetate (691860-36-3) → 4-allyl-2,6-dimethoxyphenyl (E)-cinnamate (185336-07-6)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 20 h / 20 °C

2: 2.8 g / aq. NaOH / benzene

3: 68 percent / CH₂Cl₂ / 20 °C

With sodium hydroxide; In dichloromethane; benzene;

Reference yield:

4-allyl-2,6-dimethoxyphenyl bromoacetate (691860-36-3) → 4-allyl-2,6-dimethoxyphenyl 4-coumarate

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 20 h / 20 °C

2: 2.8 g / aq. NaOH / benzene

3: 63 percent / CH₂Cl₂ / 20 °C

With sodium hydroxide; In dichloromethane; benzene;

upstream raw materials:

2-bromoacetyl chloride

4-allyl-2,6-dimethoxyphenol

Downstream raw materials:

4-allyl-2,6-dimethoxyphenyl (E)-cinnamate

(carbo-4-allyl-2,6-dimethoxyphenyloxymethylene)triphenylphosphorane

Refernces