p-chlorobenzoylmethanesulfonic acid

Base Information

• Chemical Name: p-chlorobenzoylmethanesulfonic acid
• CAS No.: 98554-12-2
• Molecular Formula: C₈H₇ClO₄S
• Molecular Weight: 234.66
• Mol file: 98554-12-2.mol

Synonyms:p-chlorobenzoylmethanesulfonic acid

Chemical Property of p-chlorobenzoylmethanesulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of p-chlorobenzoylmethanesulfonic acid

There total 1 articles about p-chlorobenzoylmethanesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

para-chloroacetophenone (99-91-2) → p-chlorobenzoylmethanesulfonic acid (98554-12-2)

Guidance literature:

With dioxane-SO₃; 1,2-dichloro-ethane;

Reference yield: 98.0%

p-chlorobenzoylmethanesulfonic acid (98554-12-2) → para-chlorobenzoic acid (74-11-3)

Guidance literature:

With water; sodium hydroxide; for 5h; Heating;

DOI:10.1134/S1070363213030092

Reference yield: 43.0%

p-chlorobenzoylmethanesulfonic acid (98554-12-2) → p-chlorobenzoylmethanesulfonyl chloride (1284292-44-9)

Guidance literature:

With phosphorus trichloride; for 14h; Heating;

DOI:10.1134/S1070363213030092

upstream raw materials:

para-chloroacetophenone

Downstream raw materials:

p-chlorobenzoylmethanesulfonyl chloride

methyl 2-methoxy-(p-chlorostyryl)sulfonate

para-chlorobenzoic acid

methyl p-chlorobenzoylmethanesulfonate

Refernces