diphenyldiboronic acid

Base Information

• Chemical Name: diphenyldiboronic acid
• CAS No.: 2848-16-0
• Molecular Formula: C₁₂H₁₂B₂O₃
• Molecular Weight: 225.847
• Mol file: 2848-16-0.mol

Synonyms:diphenyldiboronic acid

Chemical Property of diphenyldiboronic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of diphenyldiboronic acid

There total 3 articles about diphenyldiboronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-bromo-benzaldehyde (1122-91-4) + phenylboronic acid (98-80-6) → diphenyldiboronic acid (2848-16-0) + 4-Phenylbenzaldehyde (3218-36-8)

Guidance literature:

With potassium carbonate; calated clay; tetraphenylphosphonium bromide inter; palladium dichloride; In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1016/S0040-4039(98)02403-4

Reference yield:

iodobenzene (591-50-4) + phenylboronic acid (98-80-6) → biphenyl (92-52-4,1594-86-1) + diphenyldiboronic acid (2848-16-0)

Guidance literature:

With potassium carbonate; calated clay; tetraphenylphosphonium bromide inter; palladium dichloride; In N,N-dimethyl-formamide; for 1h; Heating;

DOI:10.1016/S0040-4039(98)02403-4

Reference yield:

7-bromonaphthalen-2-ol (116230-30-9) + phenylboronic acid (98-80-6) → 7-phenylnaphthalen-2-ol (221018-05-9) + diphenyldiboronic acid (2848-16-0)

Guidance literature:

With potassium carbonate; calated clay; tetraphenylphosphonium bromide inter; palladium dichloride; In N,N-dimethyl-formamide; for 2h; Heating;

DOI:10.1016/S0040-4039(98)02403-4

upstream raw materials:

4-bromo-benzaldehyde

phenylboronic acid

iodobenzene

7-bromonaphthalen-2-ol

Downstream raw materials:

4,4,6-trimethyl-2-phenyl-[1,3,2]dioxaborinane

2,6-dimethoxy-3-((S)-2-phenyl-7,8-dihydro-6H-[1,3,2]dioxaborolo[4,5-g]chromen-7-yl)-phenol

phenylboronic acid 1,2-propanediol ester

2-phenyl-4,4,5,5-tetramethyl-1,3,2-dioxoborole

Refernces