ALLYLTRIMETHYLGERMANE

Base Information Edit

Chemical Name:ALLYLTRIMETHYLGERMANE
CAS No.:762-66-3
Molecular Formula:C6H14Ge
Molecular Weight:158.767
Hs Code.:
Mol file:762-66-3.mol

Synonyms:Germane,allyltrimethyl- (6CI,7CI,8CI);Germane, trimethyl-2-propenyl- (9CI);Allyltrimethylgermane;

Suppliers and Price of ALLYLTRIMETHYLGERMANE

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of ALLYLTRIMETHYLGERMANE Edit

Chemical Property:

Vapor Pressure:22mmHg at 25°C
Refractive Index:1.4333
Boiling Point:116.1 °C at 760 mmHg
Flash Point:12.2 °C
PSA：0.00000
Density:0,995 g/cm3
LogP:2.51060

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 11
Safety Statements: 9-16-33

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ALLYLTRIMETHYLGERMANE

There total 4 articles about ALLYLTRIMETHYLGERMANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76054-64-3
7,7-dimethyl-1,4,5,6-tetraphenyl-2,3-benzo-7-germanorbornadiene

: 106-95-6
allyl bromide

: 762-66-3
allyltrimethylgermane

Guidance literature:: With CH₃MgBr; In diethyl ether; pentane; benzene; byproducts: tetraphenylnaphthalene; Norbornadiene-compound and allyl bromide are heated at 25°C for 4 h in benzene, after distilling of volatiles the residue is stirred in pentane at room temp. for 1.5 h, then methylation (MeMgBr in Et2O, 0°C (0.5 h), room temp. (1 h)) (Ar).; pptn. of tetraphenylnaphthalene, the mixture containing ether, benzene and CH2CHCH2GeMe3 is separated by distilling in vac. at room temp. and collecting in a trap cooled with dry ice, removal of ether by using a microcolumn, detected by (1)H NMR, GC-MS;

Reference yield:

: 76054-64-3
7,7-dimethyl-1,4,5,6-tetraphenyl-2,3-benzo-7-germanorbornadiene

: 107-05-1
3-chloroprop-1-ene

: 762-66-3
allyltrimethylgermane

Guidance literature:: With CH₃MgCl; In diethyl ether; benzene; Norbornadiene-compound and allyl chloride are heated at 70°C for 4 h in benzene, followed by methylation with MeMgCl in Et2O (stirring of reaction mixture at 0°C for 0.5 h, then stirring at room temp. for 1 h) (Ar).; All volatile compounds are separated by distilling in vac. at room temp. and collecting in a trap cooled with dry ice, removal of ether, residue contains traces of ether and benzene, detected by (1)H NMR and GC-MS.;