2,4-dichloro-5-methyl-benzophenone

Base Information

• Chemical Name: 2,4-dichloro-5-methyl-benzophenone
• CAS No.: 16444-45-4
• Molecular Formula: C₁₄H₁₀Cl₂O
• Molecular Weight: 265.139
• Mol file: 16444-45-4.mol

Synonyms:2,4-dichloro-5-methyl-benzophenone

Chemical Property of 2,4-dichloro-5-methyl-benzophenone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-dichloro-5-methyl-benzophenone

There total 2 articles about 2,4-dichloro-5-methyl-benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

2,4-dichlorotoluene (95-73-8) + benzoyl chloride (98-88-4) → 2,4-dichloro-5-methyl-benzophenone (16444-45-4)

Guidance literature:

With aluminium trichloride; In carbon disulfide; for 72h; Heating;

DOI:10.1055/s-1996-4344

Reference yield:

→ 2,4-dichloro-5-methyl-benzophenone (16444-45-4)

Guidance literature:

5-Methyl-2,4-dichlor-benzoesaeure, 1. Thionylchlorid, 2. Bzl., (auf dem Dampfbad);

Reference yield: 77.0%

2,4-dichloro-5-methyl-benzophenone (16444-45-4) → 3-methyl benzophenone (643-65-2)

Guidance literature:

With potassium hydroxide; hydrogen; Aliquat 336; palladium on activated charcoal; In 2,2,4-trimethylpentane; at 30 ℃; for 4.5h; under 760 Torr;

DOI:10.1055/s-1996-4344

upstream raw materials:

2,4-dichlorotoluene

benzoyl chloride

Downstream raw materials:

3-methyl benzophenone

Refernces