S-methyl nonanethioate

Base Information

• Chemical Name: S-methyl nonanethioate
• CAS No.: 86211-08-7
• Molecular Formula: C₁₀H₂₀OS
• Molecular Weight: 188.334
• Mol file: 86211-08-7.mol

Synonyms:S-methyl nonanethioate

Chemical Property of S-methyl nonanethioate

Chemical Property:

Purity/Quality:

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Technology Process of S-methyl nonanethioate

There total 14 articles about S-methyl nonanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

thiophene-2-carbothioic acid S-methyl ester (5365-44-6) + octyl p-cyanophenylmethyl ketone (1387574-33-5) → S-methyl nonanethioate (86211-08-7) + 4-<(2-Thienylcarbonyl)methyl>benzonitril (90013-81-3)

Guidance literature:

With RhH(CO)(PPh₃)3; o-phenylenebis(diphenylphosphine); In 1,3-dimethyl-2-imidazolidinone; at 150 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol3017148

Reference yield: 80.0%

4-tert-Butyl-thiobenzoesaeure-S-methylester (39274-35-6) + octyl p-cyanophenylmethyl ketone (1387574-33-5) → 4-[2-[4-(1,1-dimethylethyl)phenyl]-2-oxoethyl]benzonitrile (727722-43-2) + S-methyl nonanethioate (86211-08-7)

Guidance literature:

With RhH(CO)(PPh₃)3; o-phenylenebis(diphenylphosphine); In 1,3-dimethyl-2-imidazolidinone; at 150 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol3017148

Reference yield: 76.0%

octyl p-cyanophenylmethyl ketone (1387574-33-5) + methyl (4-methoxyphenyl)methanethionate (5925-72-4) → 4-[2-(4-methoxyphenyl)-2-oxoethyl]benzonitrile (62066-32-4) + S-methyl nonanethioate (86211-08-7)

Guidance literature:

With RhH(CO)(PPh₃)3; o-phenylenebis(diphenylphosphine); In 1,3-dimethyl-2-imidazolidinone; at 150 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol3017148

upstream raw materials:

S-Methyl 3,5-dimethoxybenzothioate

octyl p-cyanophenylmethyl ketone

C₁₂H₁₀OS

furane-2-monocarboxylic acid S-methylester

Downstream raw materials:

(S)-methyl thiobenzoate

1-phenyl-2-decanone

ethyl 4-(2-oxodecyl)benzoate

octyl p-cyanophenylmethyl ketone

Refernces