Technology Process of 1-Adamantanecarbonitrile
There total 61 articles about 1-Adamantanecarbonitrile which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thiophosphorylated amine resin; 1-ethyl-3-methylimidazolium hexafluorophosphate;
In
toluene;
at 200 ℃;
for 0.25h;
microwave irradiation;
DOI:10.1039/b008814p
- Guidance literature:
-
With
potassium hexafluorophosphate; tert.-butylnitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; 1,1,1,3,3,3-hexamethyl-disilazane;
In
acetonitrile;
at 30 ℃;
for 8h;
Temperature;
Concentration;
Sealed tube;
- Guidance literature:
-
With
chloro-trimethyl-silane;
sodium iodide;
In
N,N-dimethyl-formamide; acetonitrile;
at 60 - 65 ℃;
for 6h;
DOI:10.1021/jo00327a034
Xn,
Xi
