{(CH₃)2N}2GeCl₂

Base Information

• Chemical Name: {(CH₃)2N}2GeCl₂
• CAS No.: 24422-24-0
• Molecular Formula: C₄H₁₂Cl₂GeN₂
• Molecular Weight: 231.649
• Mol file: 24422-24-0.mol

Synonyms:{(CH₃)2N}2GeCl₂

Chemical Property of {(CH₃)2N}2GeCl₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of {(CH₃)2N}2GeCl₂

There total 2 articles about {(CH₃)2N}2GeCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

GeCl3[N(CH3)2] (24422-23-9) → germaniumtetrachloride (10038-98-9) + {(CH3)2N}2GeCl2 (24422-24-0)

Guidance literature:

In benzene;

DOI:10.1039/DT9810001264

Reference yield:

bis(dimethylamino)dimethylsilane (3768-58-9) + germaniumtetrachloride (10038-98-9) → (N,N-dimethylamino)dimethylchlorosilane (18209-60-4) + {(CH3)2N}2GeCl2 (24422-24-0)

Guidance literature:

In benzene;

DOI:10.1039/DT9810001264

Reference yield: 55.0%

(C6F5NHCH2CH2)2NCH3 (282726-67-4) + {(CH3)2N}2GeCl2 (24422-24-0) → CH3N(CH2CH2NC6F5)2GeCl2 (1176086-77-3)

Guidance literature:

In neat (no solvent); (Ar, Schlenk) a mixt. of Ge-compound and amine was heated at 130°C for 25 h, toluene was added at room temp.; filtered, washed with cold diethyl ether and dried in vac.;

DOI:10.1039/b901885a

upstream raw materials:

GeCl₃[N(CH₃)2]

bis(dimethylamino)dimethylsilane

germaniumtetrachloride

Downstream raw materials:

bis(dimethylamino)dimethylsilane

germaniumtetrachloride

CH₃N(CH₂CH₂NC₆F₅)2GeCl₂

Refernces