Diisopropylphosphinic acid p-nitrophenyl ester

Base Information

• Chemical Name: Diisopropylphosphinic acid p-nitrophenyl ester
• CAS No.: 7284-67-5
• Molecular Formula: C₁₂H₁₈NO₄P
• Molecular Weight: 271.253
• Mol file: 7284-67-5.mol

Synonyms:Diisopropyl-phosphinsaeure-(4-nitro-phenylester);1-di(propan-2-yl)phosphoryloxy-4-nitrobenzene;

Chemical Property of Diisopropylphosphinic acid p-nitrophenyl ester

Chemical Property:

• Vapor Pressure: 2.76E-05mmHg at 25°C
• Boiling Point: 368.1°C at 760 mmHg
• Flash Point: 176.4°C
• PSA: 81.93000
• Density: 1.165g/cm³
• LogP: 4.59170

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Diisopropylphosphinic acid p-nitrophenyl ester

There total 4 articles about Diisopropylphosphinic acid p-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diisopropylphosphinic acid (680-03-5) → Diisopropyl-phosphinsaeure-(4-nitro-phenylester) (7284-67-5)

Guidance literature:

Multi-step reaction with 2 steps

1: PCl₅

2: diethyl ether; triethylamine

With diethyl ether; phosphorus pentachloride; triethylamine;

Reference yield:

4-nitro-phenol (100-02-7,78813-13-5,89830-32-0) + diisopropylphosphoryl chloride (1112-15-8) → Diisopropyl-phosphinsaeure-(4-nitro-phenylester) (7284-67-5)

Guidance literature:

With diethyl ether; triethylamine;

Reference yield:

diisopropylphosphoryl chloride (1112-15-8) + 4-(4-nitrophenoxy)butanoic acid (28341-54-0) → Diisopropyl-phosphinsaeure-(4-nitro-phenylester) (7284-67-5)

Guidance literature:

With diethyl ether;

upstream raw materials:

4-nitro-phenol

diisopropylphosphoryl chloride

4-(4-nitrophenoxy)butanoic acid

diisopropylphosphinic acid