Technology Process of grassypeptolide A
There total 2 articles about grassypeptolide A which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
ammonium acetate; zinc;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/chem.201203667
- Guidance literature:
-
Multi-step reaction with 2 steps
1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 - -50 °C / Inert atmosphere
2: zinc; ammonium acetate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
With
diethylamino-sulfur trifluoride; ammonium acetate; zinc;
In
tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201203667
- Guidance literature:
-
grassypeptolide A;
With
ruthenium trichloride; sodium periodate;
In
tetrachloromethane; water; acetonitrile;
at 20 ℃;
for 1h;
With
hydrogenchloride;
In
water;
at 110 ℃;
for 16h;
Inert atmosphere;
DOI:10.1021/jo1013564
