DECYL METHANE SULFATE

Base Information

• Chemical Name: DECYL METHANE SULFATE
• CAS No.: 41233-29-8
• Molecular Formula: C11H24 O3 S
• Molecular Weight: 236.376
• Hs Code.: 2905199090
• Mol file: 41233-29-8.mol

Synonyms:1-(Methanesulfonyloxy)decane;1-Decyl mesylate; Decyl mesylate; Decyl methanesulfonate

Chemical Property of DECYL METHANE SULFATE

Chemical Property:

• Vapor Pressure: 0.000164mmHg at 25°C
• Boiling Point: 340.9°Cat760mmHg
• Flash Point: 160°C
• PSA: 51.75000
• Density: 0.995g/cm³
• LogP: 4.18410
• Storage Temp.: −20°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DECYL METHANE SULFATE

There total 4 articles about DECYL METHANE SULFATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1-Decanol (112-30-1) + methanesulfonyl chloride (124-63-0) → methanesulfonic acid decyl ester (41233-29-8)

Guidance literature:

1-Decanol; With triethylamine; In dichloromethane; at 25 ℃;

methanesulfonyl chloride; In dichloromethane; at 0 - 20 ℃;

Reference yield:

1-Decanol (112-30-1) → methanesulfonic acid decyl ester (41233-29-8)

Guidance literature:

In 2,3,5-trimethyl-pyridine; hexane;

Reference yield:

methyl undecanoate (1731-86-8) → methanesulfonic acid decyl ester (41233-29-8)

Guidance literature:

Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: pyridine / 24 h / 0 - 20 °C

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;

DOI:10.1080/14786419.2019.1686370

upstream raw materials:

1-Decanol

methanesulfonyl chloride

methyl undecanoate

Downstream raw materials:

glycerol 1-O-decylether

1-azidodecane

4-decyl-piperazine-1-carboxylic acid ethyl ester

2-(n-Decylamino)ethanol

Refernces

• 1、 Blesic, Marijana,Swadzba-Kwasny, Malgorzata,Holbrey, John D.,Canongia Lopes, Jose N.,Seddon, Kenneth R.,Rebelo, Luis Paulo N.. "New catanionic surfactants based on 1-alkyl-3-methylimidazolium alkylsulfonates, [CnH2n+1mim][CmH 2m+1SO3]: Mesomorphism and aggregation". . p. 4260 - 4268. Retrieved 2009.
• 2、 -. "Synthesis method of special-pulling universal intermediate (by machine translation)". Paragraph 0024; 0039-0042. . Retrieved 2020/06/20.
• 3、 Guan, Dongliang,Chen, Feifei,Xiong, Lun,Tang, Feng,Faridoon,Qiu, Yunguang,Zhang, Naixia,Gong, Likun,Li, Jian,Lan, Lefu,Huang, Wei. "Extra Sugar on Vancomycin: New Analogues for Combating Multidrug-Resistant Staphylococcus aureus and Vancomycin-Resistant Enterococci". supporting information. p. 286 - 304. Retrieved 2018/02/10.