(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Base Information Edit

Chemical Name:(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone
CAS No.:67119-85-1
Molecular Formula:C₉H₁₄O₂
Molecular Weight:154.209
Hs Code.:
Mol file:67119-85-1.mol

Synonyms:(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Suppliers and Price of (+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone Edit

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

There total 5 articles about (+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 488787-31-1
6-[(1-hydroxy-1-methyl)ethyl]-3-ethoxy-2-cyclohexen-1-one

: 67119-85-1
(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Guidance literature:: 6-[(1-hydroxy-1-methyl)ethyl]-3-ethoxy-2-cyclohexen-1-one; With C₆H₁₆AlO₄^(1-)*Na⁽¹⁺⁾; In tetrahydrofuran; at 0 - 20 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; at 20 ℃; for 1.5h; Inert atmosphere;

Reference yield:

: 104841-04-5
2-(2-Methoxy-4-trimethylsilanyloxy-cyclohex-3-enyl)-propan-2-ol

: 67119-85-1
(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Guidance literature:: With trichloroacetic acid; In tetrachloromethane; for 5h; Yield given; Heating;
DOI:10.1021/jo00024a031

Reference yield:

: 67119-82-8
1-(2-Methoxy-4-trimethylsilanyloxy-cyclohex-3-enyl)-ethanone

: 67119-85-1
(+/-)-4-(1-hydroxy-1-methylethyl)cyclohex-2-enone

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 1 h / Ambient temperature

2: 2percent Cl₃CCOOH / CCl₄ / 5 h / Heating

With trichloroacetic acid; In tetrachloromethane; diethyl ether;
DOI:10.1021/jo00024a031